Synthesis of Diastereomeric Spirocyclic Nitroxyl Radicals of 3-Imidazoline Series with Two Mesogenic Groups

Synthesis of Diastereomeric Spirocyclic Nitroxyl Radicals of 3-Imidazoline Series with Two Mesogenic Groups Full article

Journal

Chemistry of Heterocyclic Compounds
ISSN: 0009-3122 , E-ISSN: 1573-8353

Output data

Year: 2014, Volume: 50, Number: 8, Pages: 1113-1125 Pages count : DOI: 10.1007/s10593-014-1571-7

Tags

4-hydroxycyclohexanone; 3-imidazolines; spirocyclic nitroxyl radicals; condensation; Mitsunobu acylation

Authors

Zaitseva E. V. ¹ , Shernyukov A. V. ¹ , Amitina S. A. ¹ , Tamura R. ² , Grigor'ev I. A. ¹ , Mazhukin D. G. ^1,3

Affiliations

1	(Данные Web of science) Russian Acad Sci, Siberian Branch, NN Vorozhtsov Novosibirsk Inst Organ Chem, Novosibirsk 630090, Russia
2	(Данные Web of science) Kyoto Univ, Grad Sch Human & Environm Studies, Sakyo Ku, Yoshida Nihonmatsu, Kyoto 6068501, Japan
3	(Данные Web of science) Novosibirsk State Univ, Novosibirsk 630090, Russia

Alkylaromatic alpha-hydroxylamino ketones with a p-hydroxy(alkoxy)aryl substituent were used for the preparation of stable diastereomeric spirocyclic nitroxyl radicals of 3-imidazoline series, having two different or identical mesogenic groups in the molecule. The molecular structure of these compounds was determined by NMR study of their diamagnetic reduced derivatives.

Zaitseva E.V. , Shernyukov A.V. , Amitina S.A. , Tamura R. , Grigor'ev I.A. , Mazhukin D.G.
Synthesis of Diastereomeric Spirocyclic Nitroxyl Radicals of 3-Imidazoline Series with Two Mesogenic Groups
Chemistry of Heterocyclic Compounds. 2014. V.50. N8. P.1113-1125. DOI: 10.1007/s10593-014-1571-7 WOS Scopus РИНЦ

Published online:	Oct 8, 2014
Published print:	Nov 1, 2014

Web of science	WOS:000344093400006
Scopus	2-s2.0-84921937001
Elibrary	24030915
OpenAlex	W2002277872