Analysis of F-19 and C-13 NMR spectra of tetrafluorophthalic anhydride and its derivatives

Analysis of F-19 and C-13 NMR spectra of tetrafluorophthalic anhydride and its derivatives Full article

Journal

Journal of Fluorine Chemistry
ISSN: 0022-1139

Output data

Year: 2011, Volume: 132, Number: 8, Pages: 512-515 Pages count : DOI: 10.1016/j.jfluchem.2011.04.021

Tags

Tetrafluorophthalic anhydride; N-pentafluorophenyltetrafluorophthalimide; Hexafluoroindan-1,3-dione; F-19 and C-13 NMR Spectroscopy; DFT calculations

Authors

Chuikov Igor P. ¹ , Fadeev Dmitriy S. ¹ , Mamatyuk Victor I. ¹ , Vaganova Tamara A. ¹ , Malykhin Evgenij V. ¹

Affiliations

1	(Данные Web of science) Russian Acad Sci, NN Vorozhtsov Novosibirsk Inst Organ Chem, Siberian Branch, Novosibirsk 630090, Russia

F-19 and C-13 NMR spectra of perfluorinated compounds (i.e., tetrafluorophthalic anhydride, its hydroxyland amino-derivatives. N-pentafluorophenyltetrafluorophthalimide, and hexafluoroindan-1,3-dione) were analysed. Different signals in NMR spectra were assigned based on the analysis of spin-spin coupling constants. All assignments made were further confirmed by density functional theory (DFT) calculations of C-13 chemical shifts and J(C,F) coupling constants. (c) 2011 Elsevier B.V. All rights reserved.

Chuikov I.P. , Fadeev D.S. , Mamatyuk V.I. , Vaganova T.A. , Malykhin E.V.
Analysis of F-19 and C-13 NMR spectra of tetrafluorophthalic anhydride and its derivatives
Journal of Fluorine Chemistry. 2011. V.132. N8. P.512-515. DOI: 10.1016/j.jfluchem.2011.04.021 WOS Scopus РИНЦ

Published print:

Aug 1, 2011

Web of science	WOS:000293725700002
Scopus	2-s2.0-79960142084
Elibrary	17004166
OpenAlex	W2032048498