Efficient synthesis of beta-hydroxy sulfides by microwave-promoted ring opening in (+)-3-carene trans-epoxide with sodium thiolates

Efficient synthesis of beta-hydroxy sulfides by microwave-promoted ring opening in (+)-3-carene trans-epoxide with sodium thiolates Full article

Journal

Mendeleev Communications
ISSN: 0959-9436

Output data

Year: 2011, Volume: 21, Number: 4, Pages: 192-193 Pages count : DOI: 10.1016/j.mencom.2011.07.006

Authors

Agafontsev Alexander M. ¹ , Gorshkov Nikolay B. ¹ , Tkachev Alexey V. ^1,2

Affiliations

1	(Данные Web of science) Russian Acad Sci, NN Vorozhtsov Novosibirsk Inst Organ Chem, Siberian Branch, Novosibirsk 630090, Russia
2	(Данные Web of science) Novosibirsk State Univ, Dept Nat Sci, Novosibirsk 630090, Russia

Reaction of (+)-3-carene trans-epoxide with sodium thiolates in methanolic solution in a microwave oven at 140 degrees C for 35-40 min affords corresponding (1S,3S,4S,6R)-4-sulfanylcaran-3-ols in 75-95% yields.

Agafontsev A.M. , Gorshkov N.B. , Tkachev A.V.
Efficient synthesis of beta-hydroxy sulfides by microwave-promoted ring opening in (+)-3-carene trans-epoxide with sodium thiolates
Mendeleev Communications. 2011. V.21. N4. P.192-193. DOI: 10.1016/j.mencom.2011.07.006 WOS Scopus РИНЦ

Published print:

Jul 1, 2011

Web of science	WOS:000294095500006
Scopus	2-s2.0-79960793848
Elibrary	43197047
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