Synthesis of 1-[4-(1,3-diaryl-4,5-dihydro-1H-pyrazol-5-yl)-2,3,5,6-tetrafluorophenyl]piperidin-4-ols and their acrylates

Synthesis of 1-[4-(1,3-diaryl-4,5-dihydro-1H-pyrazol-5-yl)-2,3,5,6-tetrafluorophenyl]piperidin-4-ols and their acrylates Full article

Journal

Russian Journal of Organic Chemistry
ISSN: 1070-4280 , E-ISSN: 1608-3393

Output data

Year: 2017, Volume: 53, Number: 3, Pages: 398-406 Pages count : 9 DOI: 10.1134/S1070428017030149

Authors

Soboleva E.A. ¹ , Orlova N.A. ¹ , Shelkovnikov V.V. ^1,2

Affiliations

1	(Данные Web of science) Russian Acad Sci, Siberian Branch, Vorozhtsov Novosibirsk Inst Organ Chem, Pr Akad Lavrenteva 9, Novosibirsk 630090, Russia
2	(Данные Web of science) Novosibirsk State Tech Univ, Pr Karla Marksa 20, Novosibirsk 630073, Russia

(4-Hydroxypiperidin-1-yl)tetra- and -octafluorochalcones reacted with phenylhydrazine in acetic acid to give mixtures of polyfluoro-1,3,5-triaryl-4,5-dihydro-1H-pyrazoles and their O-acetyl derivatives. Analogous reactions in ethanol afforded in satisfactory yields 1-[4-(1,3-diaryl-4,5-dihydro-1H-pyrazol-5-yl)-2,3,5,6-tetrafluorophenyl]piperidin-4-ols which were treated with acryloyl chloride to obtain the corresponding acrylates that are promising as monomers for the preparation of fluorescent films.

Soboleva E.A. , Orlova N.A. , Shelkovnikov V.V.
Synthesis of 1-[4-(1,3-diaryl-4,5-dihydro-1H-pyrazol-5-yl)-2,3,5,6-tetrafluorophenyl]piperidin-4-ols and their acrylates
Russian Journal of Organic Chemistry. 2017. V.53. N3. P.398-406. DOI: 10.1134/S1070428017030149 WOS Scopus РИНЦ

Соболева Е.А. , Орлова Н.А. , Шелковников В.В.
Синтез 1-[4-(1,3-диарил-4,5-дигидро-1я-пиразол-5-ил)-2,3,5,6-тетра-фторфенил]пиперидин-4-олов и их акрилатов
Журнал органической химии (RUSS J ORG CHEM+). 2017. Т.53. №3. С.400-407. РИНЦ

Published print:	Mar 1, 2017
Published online:	May 5, 2017

Web of science	WOS:000400771300014
Scopus	2-s2.0-85018793922
Elibrary	31016406
OpenAlex	W2610965554