N-Lauroylsarcosine capped silver nanoparticle based inks for flexible electronics

N-Lauroylsarcosine capped silver nanoparticle based inks for flexible electronics Full article

Journal

Journal of Materials Science: Materials in Electronics
ISSN: 0957-4522 , E-ISSN: 1573-482X

Output data

Year: 2017, Volume: 28, Number: 2, Pages: 2029-2036 Pages count : 8 DOI: 10.1007/s10854-016-5762-0

Authors

Titkov Alexander I. ¹ , Bulina Natalia V. ¹ , Ulihin Artem S. ¹ , Shundrina Inna K. ^1,2 , Karpova Elena V. ² , Gerasimov Eugeny Yu. ^1,3 , Yukhin Yury.M. ¹ , Lyakhov Nikolai.Z. ¹

Affiliations

1	(Данные Web of science) Russian Acad Sci, Siberian Branch, Inst Solid State Chem & Mechanochem, Kutateladze 18, Novosibirsk 630128, Russia
2	(Данные Web of science) Russian Acad Sci, Siberian Branch, NN Vorozhtsov Novosibirsk Inst Organ Chem, Prospekt Akad Lavrentieva 9, Novosibirsk 630090, Russia
3	(Данные Web of science) Russian Acad Sci, Siberian Branch, Boreskov Inst Catalysis, Pr Acad Lavrentieva 5, Novosibirsk 630090, Russia

Silver nanoparticles stabilized by an amino and fatty acid (C12) derivative-n-lauroylsarcosine with the average size of 8.4 nm have been obtained via the reduction of the silver nitrate with hydrazine in o-xylene at room temperature. The synthesized silver nanoparticles were investigated by transmission electron microscopy, powder X-ray diffraction, UV-Vis- and IR-spectroscopy. Thermal decomposition and removal of the capping agent from the surface of the nanoparticles have been studied by thermogravimetric analysis. It was determined that n-lauroylsarcosine is removed from the surface of the nanoparticles in two stages at a temperature range of 110-210 degrees C. Ink consisting of the silver nanoparticles capped with n-nauroylsarcosine has been prepared in o-xylene. Its physical properties and stability have been studied. Silver layers were formed by spin coating the developed ink on a polyimide substrate. The structure and electrical properties of the conductive films obtained at different curing temperatures have been studied. It was found that, after annealing at various temperatures in the range of 100-250 degrees C, the deposited layers have the different structures, which determine the electrical properties. In the case of the n-lauroylsarcosine capped silver nanoparticles, low resistivity of the film (<10 mu Omega x cm) is achieved at lower temperatures (130-150 degrees C) as compared to that reported earlier for nanoparticles stabilized by fatty acids with the similar carbon chain lengths.

Titkov A.I. , Bulina N.V. , Ulihin A.S. , Shundrina I.K. , Karpova E.V. , Gerasimov E.Y. , Yukhin Y.M. , Lyakhov N.Z.
N-Lauroylsarcosine capped silver nanoparticle based inks for flexible electronics
Journal of Materials Science: Materials in Electronics. 2017. V.28. N2. P.2029-2036. DOI: 10.1007/s10854-016-5762-0 WOS Scopus РИНЦ

Published online:	Oct 5, 2016
Published print:	Jan 1, 2017

Web of science	WOS:000394232600115
Scopus	2-s2.0-84990864931
Elibrary	29466976
OpenAlex	W2527942083