Determination of boron in organic compounds by microwave plasma-atomic emission spectrometry

Determination of boron in organic compounds by microwave plasma-atomic emission spectrometry Full article

Journal

Journal of Analytical Chemistry
ISSN: 1061-9348 , E-ISSN: 1608-3199

Output data

Year: 2016, Volume: 71, Number: 11, Pages: 1089-1095 Pages count : DOI: 10.1134/S1061934816090033

Tags

boron-containing organic compounds; sample preparation; microwave plasma atomic emission spectrometry

Authors

Bazhenov M. A. ^1,2 , Tikhova V. D. ¹ , Fadeeva V. P. ^1,2

Affiliations

1	(Данные Web of science) Russian Acad Sci, Novosibirsk Organ Chem Inst, Siberian Branch, Novosibirsk 630090, Russia
2	(Данные Web of science) Novosibirsk Natl Res State Univ, Novosibirsk 630090, Russia

We propose a method for the determination of boron in aliphatic and aromatic trifluoroborates (including perfluorinated ones), ethers, and organoboron compounds containing dioxoborolane fragments, pyridine, and pyrazole rings, and triple bonds. The substances were decomposed by the oxygen flask combustion method. Boron was determined on an Agilent 4100 microwave plasma-atomic emission spectrometer. A number of organic compounds were analyzed, and the mass fraction of boron was determined with an error less than +/- 0.3 abs. %.

Bazhenov M.A. , Tikhova V.D. , Fadeeva V.P.
Determination of boron in organic compounds by microwave plasma-atomic emission spectrometry
Journal of Analytical Chemistry. 2016. V.71. N11. P.1089-1095. DOI: 10.1134/S1061934816090033 WOS Scopus РИНЦ

Published print:	Nov 1, 2016
Published online:	Nov 5, 2016

Web of science	WOS:000387406800003
Scopus	2-s2.0-85013774293
Elibrary	29481274
OpenAlex	W2548145250