Microwave-Assisted Synthesis of Phthalocyanine Zinc Complexes Derived from Aminotricyanobiphenyl-Based Azo Dyes

Microwave-Assisted Synthesis of Phthalocyanine Zinc Complexes Derived from Aminotricyanobiphenyl-Based Azo Dyes Full article

Journal

Macroheterocycles
ISSN: 1998-9539

Output data

Year: 2016, Volume: 9, Number: 1, Pages: 80-88 Pages count : 9 DOI: 10.6060/mhc151192s

Tags

Azo compounds; zinc complexes of phthalocyanine; microwave assistance

Authors

Selivanova Galina A. ¹ , Amosov Evgeny V. ¹ , Vasilyev Vladimir G. ¹ , Lukyanets Evgeny A. ² , Tretyakov Evgeny V. ¹ , Shteingarts Vitalij D. ¹

Affiliations

1	(Данные Web of science) Russian Acad Sci, Siberian Branch, NN Vorozhtsov Novosibirsk Inst Organ Chem, Novosibirsk 630090, Russia
2	(Данные Web of science) Res Inst Organ Intermediates & Dyes, Moscow 123995, Russia

Several new azo compounds were obtained by coupling 2,3',4'-tricyanodipherly1-4-diazonium bisulfate with beta-napthol beta-naphthol, 3-hyfroxy-2-naphthoic and acids, aniline, 2-toluidine, 2,6-xylidine, and,V, IV-dibutylaniline. New zinc complexes of tetra-4-1:2-cyano-4-(2-hydroxy-l-naphthyldiazenyl)plielphtlialocyanine and tetra-4-1:2-cyano-444dibutylaminophenyldiazenyl)phenyll-phthalocyanine were obtained in 84 % and 67 % yields by condensation of the corresponding azo compounds in the presence of zinc acetate under microwave assistance. This method was also succe.slittly applied fix the preparation of known zinc complexes based on 4-substituted 2,3 ',4'-tricyanodiphenyls with enhanced yields.

Selivanova G.A. , Amosov E.V. , Vasilyev V.G. , Lukyanets E.A. , Tretyakov E.V. , Shteingarts V.D.
Microwave-Assisted Synthesis of Phthalocyanine Zinc Complexes Derived from Aminotricyanobiphenyl-Based Azo Dyes

Macroheterocycles. 2016. V.9. N1. P.80-88. DOI: 10.6060/mhc151192s WOS Scopus РИНЦ

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