Plant coumarins: XIII. Synthesis of 2,3,9-trisubstituted furocoumarins Full article
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Russian Journal of Organic Chemistry
ISSN: 1070-4280 , E-ISSN: 1608-3393 |
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Output data | Year: 2013, Volume: 49, Number: 3, Pages: 403-411 Pages count : 9 DOI: 10.1134/S1070428013030159 | ||
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Abstract:
Peucedanin reacted with methylideneiminium salt generated in situ from N,N,N',N'-tetramethylmethanediamine and acetyl chloride to give 2-(dimethylaminomethyl)oreoselone. Reactions of peucedanin with aminomethylating agents generated in situ from formaldehyde and dimethylamine, N-methylpiperazine, or N-Boc-piperazine in boiling methanol smoothly afforded the corresponding 9-aminomethyl derivatives whose hydrolysis produced 9-aminomethyl-substituted oreoselones. 2,3,9-Trisubstituted linearly fused furocoumarins were synthesized by reactions of 9-substituted oreoselone trifluoromethanesulfonates with arylboronic acids.
Cite:
Lipeeva A.V.
, Shul'ts E.E.
, Shakirov M.M.
, Bagryanskaya I.Y.
, Tolstikov G.A.
Plant coumarins: XIII. Synthesis of 2,3,9-trisubstituted furocoumarins
Russian Journal of Organic Chemistry. 2013. V.49. N3. P.403-411. DOI: 10.1134/S1070428013030159 WOS Scopus РИНЦ OpenAlex
Plant coumarins: XIII. Synthesis of 2,3,9-trisubstituted furocoumarins
Russian Journal of Organic Chemistry. 2013. V.49. N3. P.403-411. DOI: 10.1134/S1070428013030159 WOS Scopus РИНЦ OpenAlex
Original:
Липеева А.В.
, Шульц Э.Э.
, Шакиров М.М.
, Багрянская И.Ю.
, Толстиков Г.А.
Исследование растительных кумаринов xiii. синтез 2,3,9-тризамещенных фурокумаринов
Журнал органической химии (RUSS J ORG CHEM+). 2013. Т.49. №3. С.416-424. РИНЦ
Исследование растительных кумаринов xiii. синтез 2,3,9-тризамещенных фурокумаринов
Журнал органической химии (RUSS J ORG CHEM+). 2013. Т.49. №3. С.416-424. РИНЦ
Dates:
Published print: | Mar 1, 2013 |
Published online: | Apr 6, 2013 |
Identifiers:
Web of science: | WOS:000317353500015 |
Scopus: | 2-s2.0-84879635437 |
Elibrary: | 20442292 |
OpenAlex: | W2057411734 |