Novel atom-economic synthesis of thioselenophosphinates via three-component reaction between secondary phosphine sulfides, elemental selenium, and amines Full article
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Journal of Sulfur Chemistry
ISSN: 1741-5993 |
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| Output data | Year: 2011, Volume: 32, Number: 6, Pages: 599-610 Pages count : DOI: 10.1080/17415993.2011.628993 | ||||
| Tags | amines; secondary phosphine sulfides; elemental selenium; thioselenophosphinates; three-component reaction | ||||
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Abstract:
An efficient, general, and atom-economic synthesis of organoammonium thioselenophosphinates has been developed by exploiting a three-component reaction between secondary phosphine sulfides, elemental selenium, and various amines. The reaction proceeds under mild conditions (70-75 degrees C, 1 h, EtOH) to afford thioselenophosphinates in 77-94% yields. [GRAPHICS] R-1 = aryl, arylalkyl, hetarylalkyl R-2, R-3, R-4 = H, Et, Bu, Bn, All, Ph, HO(CH2)(2), (R)-CH2CH(OH) Et
Cite:
Artem'ev A.V.
, Malysheva S.F.
, Korocheva A.O.
, Gatilov Y.V.
, Mamatyuk V.I.
, Gusarova N.K.
Novel atom-economic synthesis of thioselenophosphinates via three-component reaction between secondary phosphine sulfides, elemental selenium, and amines
Journal of Sulfur Chemistry. 2011. V.32. N6. P.599-610. DOI: 10.1080/17415993.2011.628993 WOS Scopus РИНЦ OpenAlex
Novel atom-economic synthesis of thioselenophosphinates via three-component reaction between secondary phosphine sulfides, elemental selenium, and amines
Journal of Sulfur Chemistry. 2011. V.32. N6. P.599-610. DOI: 10.1080/17415993.2011.628993 WOS Scopus РИНЦ OpenAlex
Dates:
| Published online: | Nov 2, 2011 |
| Published print: | Dec 1, 2011 |
Identifiers:
| Web of science: | WOS:000299731500009 |
| Scopus: | 2-s2.0-84857241186 |
| Elibrary: | 18035380 |
| OpenAlex: | W2028478424 |