Synthesis and molecular and crystalline structure of polyfluoro-1,3-diazafluorenes Full article
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Russian Journal of Organic Chemistry
ISSN: 1070-4280 , E-ISSN: 1608-3393 |
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| Output data | Year: 2004, Volume: 40, Number: 3, Pages: 421-425 Pages count : 5 DOI: 10.1023/B:RUJO.0000034983.96937.18 | ||
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Abstract:
Reactions of 2-amino-3-(1-imino-2,2,2-trifluoroethyl)hexafluoro-1H-indene with carboxylic acid anhydrides and chlorides afforded 2-alkyl(aryl)-4-trifluoromethyl-5,6,7,8,9,9-hexafluoro-1,3-diazafluorenes. The molecular and crystalline structure of the products was studied by NMR spectroscopy and X-ray diffraction. 5,6,7,8,9,9-Hexafluoro-2-phenyl-4-trifluoromethyl-1,3-diazafluorene in crystal gives rise to infinite ladder chains via :tau-stacking interaction between the benzene ring of one molecule and tetrafluoro benzene fragment of the other.
Cite:
Karpov V.
, Platonov V.
, Chuikov I.
, Rybalova T.
, Gatilov Y.
, Shakirov M.
Synthesis and molecular and crystalline structure of polyfluoro-1,3-diazafluorenes
Russian Journal of Organic Chemistry. 2004. V.40. N3. P.421-425. DOI: 10.1023/B:RUJO.0000034983.96937.18 WOS Scopus РИНЦ OpenAlex
Synthesis and molecular and crystalline structure of polyfluoro-1,3-diazafluorenes
Russian Journal of Organic Chemistry. 2004. V.40. N3. P.421-425. DOI: 10.1023/B:RUJO.0000034983.96937.18 WOS Scopus РИНЦ OpenAlex
Original:
Карпов В.М.
, Платонов В.Е.
, Чуйков И.П.
, Рыбалова Т.В.
, Гатилов Ю.В.
, Шакиров М.М.
Синтез, молекулярная и кристаллическая структура полифтор-1,з-диазафлуоренов
Журнал органической химии (RUSS J ORG CHEM+). 2004. Т.40. №3. С.448-452. РИНЦ
Синтез, молекулярная и кристаллическая структура полифтор-1,з-диазафлуоренов
Журнал органической химии (RUSS J ORG CHEM+). 2004. Т.40. №3. С.448-452. РИНЦ
Dates:
| Published print: | Mar 1, 2004 |
Identifiers:
| Web of science: | WOS:000222375200024 |
| Scopus: | 2-s2.0-3242783311 |
| Elibrary: | 14567467 |
| OpenAlex: | W2949363349 |