Synthesis and crystal structure of a pyrazole derivative of artemisia ketone

Synthesis and crystal structure of a pyrazole derivative of artemisia ketone Full article

Journal

Chemistry of Natural Compounds
ISSN: 0009-3130 , E-ISSN: 1573-8388

Output data

Year: 2000, Volume: 36, Number: 2, Pages: 152-155 Pages count : 4 DOI: 10.1007/BF02236419

Tags

Artemisia glabella; artemisia ketone; 5-(1 ',1 '-dimethylallyl)-3,3-dimethyl-3H-pyrazole-N,N '-dioxide; synthesis

Authors

Atazhanova G.A. ¹ , Kulyyasov A.T. ¹ , Dembitskii A.D. ¹ , Raldugin V.A. ² , Shakirov M.M. ² , Bagryanskaya I.Yu. ² , Gatilov Yu.V. ² , Adekenov S.M. ¹ , Tolstikov G.A. ²

Affiliations

1	(Данные Web of science) Minist Educ & Sci, Inst Phytochem, Karanganda, Kazakhstan
2	(Данные Web of science) Russian Acad Sci, Novosibirsk Inst Org Chem, Siberian Div, Novosibirsk 630090, Russia

The oxime of artemisia ketone is smoothly converted to the pyrazole derivative by sodium nitrate and acetic acid in CHCl3. The structure of the pyrazole was found by x-ray structural analysis. The PMR and C-13 NMR spectra were interpreted using two-dimensional H-1-C-13 NMR (COSY, COLOC).

Atazhanova G.A. , Kulyyasov A.T. , Dembitskii A.D. , Raldugin V.A. , Shakirov M.M. , Bagryanskaya I.Y. , Gatilov Y.V. , Adekenov S.M. , Tolstikov G.A.
Synthesis and crystal structure of a pyrazole derivative of artemisia ketone
Chemistry of Natural Compounds. 2000. V.36. N2. P.152-155. DOI: 10.1007/BF02236419 WOS Scopus РИНЦ OpenAlex

Published print:

Mar 1, 2000

Web of science:	WOS:000165594400010
Scopus:	2-s2.0-0034144721
Elibrary:	13343639
OpenAlex:	W2019265329

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