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Thermolytic reactions of polyfluoroaromatic compounds-XI. Copyrolysis of pentafluorosubstituted derivatives of benzene with sources of difluorocarbene. Formation of perfluoroindan Full article

Journal Tetrahedron
ISSN: 0040-4020
Output data Year: 1975, Volume: 31, Number: 9, Pages: 1201-1207 Pages count : DOI: 10.1016/0040-4020(75)85057-5
Authors Malyuta N. G. , Platonov V. E. , Furin G. G. , Yakobson G. G.
Affiliations
1 (Scopus) Institute of Organic Chemistry, Novosibirsk, 630090, Russian Federation

Abstract: Copyrolysis of compounds of the type C6F5X (X OH, OCH3, SH, NH2) with sources of difluorocarbene (CF2 CF2, CHClF2 and others) in a flow system at 600-700° is shown to give perfluoroindan in high yield. Perfluorinated methylindanes, perfluorocoumaran and other compounds are also formed. From pentafluorophenol and hexafluoropropylene oxide at 250° α,α,2,3,4,5,6-heptafluoroanisole is obtained. The participation of the perfluorobenzyl radical in the formation of perfluoroindan is discussed in the reactions investigated. © 1975.
Cite: Malyuta N.G. , Platonov V.E. , Furin G.G. , Yakobson G.G.
Thermolytic reactions of polyfluoroaromatic compounds-XI. Copyrolysis of pentafluorosubstituted derivatives of benzene with sources of difluorocarbene. Formation of perfluoroindan
Tetrahedron. 1975. V.31. N9. P.1201-1207. DOI: 10.1016/0040-4020(75)85057-5 WOS Scopus OpenAlex
Dates:
Published print: Jan 1, 1975
Identifiers:
Web of science: WOS:A1975AA89100013
Scopus: 2-s2.0-0010773904
OpenAlex: W1551045661
Citing:
DB Citing
Scopus 25
Web of science 30
OpenAlex 25
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