Double complex [Mn-2(C11H13N3O)(6)(H2O)(2)][Cr(NH3)(2)(NCS)(4)](4): Synthesis and crystal structure

Double complex [Mn-2(C11H13N3O)(6)(H2O)(2)][Cr(NH3)(2)(NCS)(4)](4): Synthesis and crystal structure Full article

Journal

Russian Journal of Inorganic Chemistry
ISSN: 0036-0236

Output data

Year: 2017, Volume: 62, Number: 2, Pages: 182-186 Pages count : 5 DOI: 10.1134/S003602361702005X

Authors

Cherkasova T.G. ¹ , Bagryanskaya I.Yu. ^2,3 , Pervukhina N.V. ⁴ , Vornakov A.L. ¹ , Cherkasova E.V. ¹ , Kuratieva N.V. ^3,4

Affiliations

1	(Данные Web of science) Kuzbass State Tech Univ, Ul Vesennyaya 28, Kemerovo 650000, Russia
2	(Данные Web of science) Russian Acad Sci, Vorozhtsov Novosibirsk Inst Organ Chem, Siberian Branch, Pr Akad Lavrenteva 9, Novosibirsk 630090, Russia
3	(Данные Web of science) Novosibirsk Natl Res State Univ, Ul Pirogova 2, Novosibirsk 630090, Russia
4	(Данные Web of science) Russian Acad Sci, Siberian Branch, Nikolaev Inst Inorgan Chem, Pr Akad Lavrenteva 3, Novosibirsk 630090, Russia

[Mn-2(C11H13N3O)(6)(H2O)(2)][Cr(NH3)(2)(NCS)(4)](4) (I) has been synthesized by the reaction between MnCl2 center dot H2O, NH4[Cr(NH3)(2)(NCS)(4)] center dot 0.5H(2)O and 4-aminoantipyrine (C11H13N3O) in an aqueous solution, and its structure has been determined by IR spectroscopy and X-ray diffraction. Crystals of complex I are triclinic, space group , Z = 1, a = 13.2378(5) , b = 15.7796(5) , c = 16.7703(6) , alpha = 83.194(2)A degrees, beta = 75.874(2)A degrees, gamma = 66.529(1)A degrees, V = 3115.2(2) (3), and rho(calcd) = 1.407 g/cm(3).

Cherkasova T.G. , Bagryanskaya I.Y. , Pervukhina N.V. , Vornakov A.L. , Cherkasova E.V. , Kuratieva N.V.
Double complex [Mn-2(C11H13N3O)(6)(H2O)(2)][Cr(NH3)(2)(NCS)(4)](4): Synthesis and crystal structure
Russian Journal of Inorganic Chemistry. 2017. V.62. N2. P.182-186. DOI: 10.1134/S003602361702005X WOS Scopus РИНЦ OpenAlex

Черкасова Т.Г. , Багрянская И.Ю. , Первухина Н.В. , Ворнаков А.Л. , Черкасова Е.В. , Куратьева Н.В.
Синтез и кристаллическая структура двойного комплексного соединения [MN2(C11H13N3O)6(H2O)2][CR(NH3)2(NCS)4]4
Журнал органической химии (RUSS J ORG CHEM+). 2017. Т.623. №2. С.188-192. РИНЦ

Published print:	Feb 1, 2017
Published online:	Feb 25, 2017

Web of science:	WOS:000395029300007
Scopus:	2-s2.0-85013957500
Elibrary:	29484959
OpenAlex:	W2591214311

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