One-pot synthesis of 1,5,3-oxathiazepanes via the three-component condensation of primary amines, formaldehyde and 2-mercaptoethanol

One-pot synthesis of 1,5,3-oxathiazepanes via the three-component condensation of primary amines, formaldehyde and 2-mercaptoethanol Научная публикация

Журнал

Tetrahedron Letters
ISSN: 0040-4039

Вых. Данные

Год: 2017, Том: 58, Номер: 19, Страницы: 1868-1870 Страниц : 3 DOI: 10.1016/j.tetlet.2017.03.090

Ключевые слова

1,5,3-Oxathiazepanes; Three-component reaction; One-pot synthesis; 7-Membered heterocycles

Авторы

Kovaleva Kseniya S. ^1,2 , Yarovaya Olga I. ^1,2 , Fadeev Dmitriy S. ¹ , Salakhutdinov Nariman F. ^1,2

Организации

1	(Данные Web of science) Russian Acad Sci, Siberian Branch, NN Vorozhtsov Novosibirsk Inst Organ Chem, Lavrentjev Ave 9, Novosibirsk 630090, Russia
2	(Данные Web of science) Novosibirsk State Univ, Pirogova St 2, Novosibirsk 630090, Russia

The three-component condensation reaction of primary amines, formaldehyde and 2-mercaptoethanol using salts of transition and rare earth metals as catalysts was developed to obtain a new 7-membered heterocyclic structural building block, 1,5,3-oxathiazepanes, in good to excellent yields. The structure of the heterocyclic fragment was confirmed by NMR spectroscopy. (C) 2017 Elsevier Ltd. All rights reserved.

Kovaleva K.S. , Yarovaya O.I. , Fadeev D.S. , Salakhutdinov N.F.
One-pot synthesis of 1,5,3-oxathiazepanes via the three-component condensation of primary amines, formaldehyde and 2-mercaptoethanol
Tetrahedron Letters. 2017. V.58. N19. P.1868-1870. DOI: 10.1016/j.tetlet.2017.03.090 WOS Scopus РИНЦ

Опубликована в печати:

1 мая 2017 г.

Web of science	WOS:000401204400015
Scopus	2-s2.0-85017256448
РИНЦ	29492997
OpenAlex	W2605034778