Synthesis of Nickel Nanoparticles by the Reduction of Its Salts Using the Modified Polyol Method in the Presence of Sodium Polyacrylates with Various Molecular Weights Full article
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Russian Journal of General Chemistry
ISSN: 1070-3632 , E-ISSN: 1608-3350 |
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| Output data | Year: 2018, Volume: 88, Number: 2, Pages: 288-294 Pages count : DOI: 10.1134/S1070363218020160 | ||||
| Tags | nano nickel; sodium polyacrylate; ethylene glycol; hydrazine hydrate; reduction | ||||
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Abstract:
Nickel nanoparticles were synthesized by the reduction of its salts by hydrazine hydrate in a polyol medium in the presence of sodium polyacrylates with molecular weights of 1200, 5100, and 8000. The nanoparticles were characterized by X-ray diffraction, scanning and transmission electron microscopy, IR spectroscopy, and thermogravimetric analysis. The effect of the synthesis conditions, such as temperature, molecular weight of sodium polyacrylate, and polyol and precursor types, on the reduction products were studied. It was shown that the average particle sizes, their aggregation and polydispersity degrees increase as the polymer molecular weight increases.
Cite:
Logutenko O.A.
, Titkov A.I.
, Vorob'ev A.M.
, Shundrina I.K.
, Yukhin Y.M.
, Lyakhov N.Z.
Synthesis of Nickel Nanoparticles by the Reduction of Its Salts Using the Modified Polyol Method in the Presence of Sodium Polyacrylates with Various Molecular Weights
Russian Journal of General Chemistry. 2018. V.88. N2. P.288-294. DOI: 10.1134/S1070363218020160 WOS Scopus РИНЦ
Synthesis of Nickel Nanoparticles by the Reduction of Its Salts Using the Modified Polyol Method in the Presence of Sodium Polyacrylates with Various Molecular Weights
Russian Journal of General Chemistry. 2018. V.88. N2. P.288-294. DOI: 10.1134/S1070363218020160 WOS Scopus РИНЦ
ArticleLinkType.TRANSLATED_TO_ORIGINAL:
Логутенко О.А.
, Титков А.И.
, Воробьев А.Ю.
, Шундрина И.К.
, Юхин Ю.М.
, Ляхов Н.З.
СИНТЕЗ НАНОЧАСТИЦ НИКЕЛЯ ВОССТАНОВЛЕНИЕМ ЕГО СОЛЕЙ МОДИФИЦИРОВАННЫМ ПОЛИОЛЬНЫМ МЕТОДОМ В ПРИСУТСТВИИ ПОЛИАКРИЛАТОВ НАТРИЯ С РАЗЛИЧНОЙ МОЛЕКУЛЯРНОЙ МАССОЙ
Журнал общей химии (RUSS J GEN CHEM+). 2018. Т.88. №2. С.311-318. РИНЦ
СИНТЕЗ НАНОЧАСТИЦ НИКЕЛЯ ВОССТАНОВЛЕНИЕМ ЕГО СОЛЕЙ МОДИФИЦИРОВАННЫМ ПОЛИОЛЬНЫМ МЕТОДОМ В ПРИСУТСТВИИ ПОЛИАКРИЛАТОВ НАТРИЯ С РАЗЛИЧНОЙ МОЛЕКУЛЯРНОЙ МАССОЙ
Журнал общей химии (RUSS J GEN CHEM+). 2018. Т.88. №2. С.311-318. РИНЦ
Dates:
| Published print: | Feb 1, 2018 |
| Published online: | Mar 15, 2018 |
Identifiers:
| Web of science | WOS:000427630200016 |
| Scopus | 2-s2.0-85044174879 |
| Elibrary | 35513329 |
| OpenAlex | W2790270039 |