Synthesis of Nickel Nanoparticles by the Reduction of Its Salts Using the Modified Polyol Method in the Presence of Sodium Polyacrylates with Various Molecular Weights

Synthesis of Nickel Nanoparticles by the Reduction of Its Salts Using the Modified Polyol Method in the Presence of Sodium Polyacrylates with Various Molecular Weights Научная публикация

Журнал

Russian Journal of General Chemistry
ISSN: 1070-3632 , E-ISSN: 1608-3350

Вых. Данные

Год: 2018, Том: 88, Номер: 2, Страницы: 288-294 Страниц : DOI: 10.1134/S1070363218020160

Ключевые слова

nano nickel; sodium polyacrylate; ethylene glycol; hydrazine hydrate; reduction

Авторы

Logutenko O. A. ¹ , Titkov A. I. ¹ , Vorob'ev A. M. ¹ , Shundrina I. K. ² , Yukhin Yu. M. ¹ , Lyakhov N. Z. ¹

Организации

1	(Данные Web of science) Russian Acad Sci, Inst Solid State Chem & Mechanochem, Siberian Branch, Ul Kutateladze 18, Novosibirsk 630128, Russia
2	(Данные Web of science) Russian Acad Sci, NN Vorozhtsov Inst Organ Chem, Siberian Branch, Novosibirsk, Russia

Nickel nanoparticles were synthesized by the reduction of its salts by hydrazine hydrate in a polyol medium in the presence of sodium polyacrylates with molecular weights of 1200, 5100, and 8000. The nanoparticles were characterized by X-ray diffraction, scanning and transmission electron microscopy, IR spectroscopy, and thermogravimetric analysis. The effect of the synthesis conditions, such as temperature, molecular weight of sodium polyacrylate, and polyol and precursor types, on the reduction products were studied. It was shown that the average particle sizes, their aggregation and polydispersity degrees increase as the polymer molecular weight increases.

Logutenko O.A. , Titkov A.I. , Vorob'ev A.M. , Shundrina I.K. , Yukhin Y.M. , Lyakhov N.Z.
Synthesis of Nickel Nanoparticles by the Reduction of Its Salts Using the Modified Polyol Method in the Presence of Sodium Polyacrylates with Various Molecular Weights
Russian Journal of General Chemistry. 2018. V.88. N2. P.288-294. DOI: 10.1134/S1070363218020160 WOS Scopus РИНЦ

Логутенко О.А. , Титков А.И. , Воробьев А.Ю. , Шундрина И.К. , Юхин Ю.М. , Ляхов Н.З.
СИНТЕЗ НАНОЧАСТИЦ НИКЕЛЯ ВОССТАНОВЛЕНИЕМ ЕГО СОЛЕЙ МОДИФИЦИРОВАННЫМ ПОЛИОЛЬНЫМ МЕТОДОМ В ПРИСУТСТВИИ ПОЛИАКРИЛАТОВ НАТРИЯ С РАЗЛИЧНОЙ МОЛЕКУЛЯРНОЙ МАССОЙ
Журнал общей химии (RUSS J GEN CHEM+). 2018. Т.88. №2. С.311-318. РИНЦ

Опубликована в печати:	1 февр. 2018 г.
Опубликована online:	15 мар. 2018 г.

Web of science	WOS:000427630200016
Scopus	2-s2.0-85044174879
РИНЦ	35513329
OpenAlex	W2790270039