Perfluoro-3-ethyl-1,2,3,10b-tetrahydrofluoranthene

Perfluoro-3-ethyl-1,2,3,10b-tetrahydrofluoranthene Научная публикация

Журнал

MolBank
ISSN: 1422-8599

Вых. Данные

Год: 2024, Том: 2024, Номер: 3, Номер статьи : M1842, Страниц : DOI: 10.3390/m1842

Ключевые слова

perfluorinated; fluoranthene; fluorene; antimony pentafluoride; 19F NMR; 19F–19F COSY; 19F–19F NOESY; variable-temperature NMR

Авторы

Komarov Vladislav V. ¹ , Krasnov Vyacheslav I. ¹ , Karpov Victor M. ¹ , Parkhomenko Dmitriy A. ¹ , Mezhenkova Tatyana V. ¹

Организации

1	N. N. Vorozhtsov Novosibirsk Institute of Organic Chemistry SB RAS

The title compound was synthesized from perfluoro-1-ethyltetralin and 1,2,3,4-tetrafluorobenzene under the action of antimony pentafluoride as a mixture of cis- and trans-isomers in a 71% isolated yield. The structure and cis-/trans-configuration of the isomers were determined by NMR (19F, 13C), 19F–19F COSY, and 19F–19F NOESY 2D NMR spectroscopy.

Komarov V.V. , Krasnov V.I. , Karpov V.M. , Parkhomenko D.A. , Mezhenkova T.V.
Perfluoro-3-ethyl-1,2,3,10b-tetrahydrofluoranthene
MolBank. 2024. V.2024. N3. M1842 . DOI: 10.3390/m1842

Поступила в редакцию:	6 июн. 2024 г.
Принята к публикации:	20 июн. 2024 г.
Опубликована online:	25 июн. 2024 г.

OpenAlex

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