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One-Pot Atom-Economic Synthesis of Thioselenophosphinates via a New Multicomponent Reaction of Secondary Phosphanes with Elemental Sulfur, Selenium, and Amines Научная публикация

Журнал European Journal of Organic Chemistry
ISSN: 1434-193X , E-ISSN: 1099-0690
Вых. Данные Год: 2010, Том: 2010, Номер: 32, Страницы: 6157-6160 Страниц : DOI: 10.1002/ejoc.201001189
Ключевые слова Phosphanes; Sulfur; Selenium; Amines; Multicomponent reactions
Авторы Artem'ev Alexander V. 1 , Gusarova Nina K. 1 , Malysheva Svetlana F. 1 , Mamatyuk Victor I. 2 , Gatilov Yurii V. 2 , Ushakov Igor A. 1 , Trofimov Boris A. 1
Организации
1 (Данные Web of science) Russian Acad Sci, Siberian Branch, AE Favorsky Irkutsk Inst Chem, Irkutsk 664033, Russia
2 (Данные Web of science) Russian Acad Sci, Siberian Branch, NN Vorozhtsov Novosibirsk Inst Organ Chem, Novosibirsk 630090, Russia

Реферат: The multicomponent reaction between secondary phosphanes R2PH (R = Ph, arylalkyl, hetarylalkyl), elemental sulfur, selenium, and primary, secondary, or tertiary amines to afford the corresponding mono-, di-, and trialkylammonium thioselenophosphinates has been discovered. The atom-economic reaction proceeds under mild conditions (ethanol/toluene, 40-70 degrees C, 40 min) to give the target alkylammonium thioselenophosphinates in high yields (up to 94%).
Библиографическая ссылка: Artem'ev A.V. , Gusarova N.K. , Malysheva S.F. , Mamatyuk V.I. , Gatilov Y.V. , Ushakov I.A. , Trofimov B.A.
One-Pot Atom-Economic Synthesis of Thioselenophosphinates via a New Multicomponent Reaction of Secondary Phosphanes with Elemental Sulfur, Selenium, and Amines
European Journal of Organic Chemistry. 2010. V.2010. N32. P.6157-6160. DOI: 10.1002/ejoc.201001189 WOS Scopus РИНЦ
Даты:
Опубликована online: 11 окт. 2010 г.
Опубликована в печати: 1 нояб. 2010 г.
Идентификаторы:
Web of science WOS:000285041500005
Scopus 2-s2.0-78249272919
РИНЦ 16697762
OpenAlex W2023525548
Альметрики: